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Título: | Characterization of trimethylsilyl ethers of iminosugars by gas chromatography-mass spectrometry |
Autor: | Rodríguez-Sánchez, Sonia CSIC; Ruiz-Matute, Ana I. CSIC ORCID ; Sanz, M. Luz CSIC ORCID ; Soria, Ana C. CSIC ORCID | Palabras clave: | Trimethylsilylation Mass spectrometry Linear retention indices Gas chromatography Iminosugars Aglaonema treubii |
Fecha de publicación: | 2014 | Citación: | Journal of chromatography. A 1372: 221-227 (2014) | Resumen: | A combination of gas chromatographic retention data (linear retention indices) on two different stationary phases (100% methyl- and 50% phenylmethylsilicone) and electron impact mass spectrometric relative abundances for characteristic m/z ratios of 12 trimethylsilylated piperidine and pyrrolidine iminosugars are reported. These results have been related to their structural features and applied to the characterization of iminosugar composition of an Aglaonema treubii root extract. Seven iminosugars were detected in this extract, two of them were described for the first time. | URI: | http://hdl.handle.net/10261/109473 | DOI: | 10.1016/j.chroma.2014.10.084 | Identificadores: | doi: 10.1016/j.chroma.2014.10.084 issn: 0021-9673 e-issn: 1873-3778 |
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